基于动态测试的维卡软化温度测定仪校准装置研制
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河北省计量监督检测研究院 石家庄 050051

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TN98

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Development of calibration device for vicat softening point tester based on dynamic testing
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Hebei Provincial Institute of Metrology Supervision and Testing,Shijiazhuang 050051, China

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    摘要:

    维卡软化温度测定仪长期使用后,常出现温度示值偏差与升温速率不准的问题。为此,研究开发了一套基于动态测试原理的高精度校准装置。这套装置配备自动触发式图像采集温度记录装置,当试样发生1 mm变形或被压针刺入的瞬间,能实时捕捉形变临界点,精准记录温度。其工作流程包含试样放置、参数设定等环节,各环节衔接顺畅。实际测试中,该装置表现出明显优势:12℃/6 min升温速率下,实际升温速率在(11.9~12.1)℃/6 min之间,温度示值误差为(-0.1~0.2)℃;5℃/6 min升温速率下,实际升温速率处于(4.9~5.1)℃/6 min 范围,温度示值误差(-0.1~0.2)℃,均符合技术要求。经分析,温度示值误差标准不确定度为0.067℃,升温速率误差标准不确定度为0.091℃/h。研究的创新点体现在提出动态升温校准方法,优化动态采集策略,将智能校准算法与自动化流程集成,可支持多温度点、多样品站同步校准。该装置有效解决了现有校准方法存在的问题,实现了温度与升温速率的同步动态精准测量,为材料热性能测试提供了可靠保障,在材料研发、质量控制等领域发挥着重要作用。

    Abstract:

    After long-term use of Vicat softening temperature testers, problems such as temperature indication deviation and inaccurate heating rate often occur. To address this, a high-precision calibration device based on the principle of dynamic testing has been developed. This device is equipped with an auto-triggered image acquisition and temperature recording device, which can real-time capture the deformation critical point and accurately record the temperature at the moment when the sample undergoes a 1 mm deformation or is pierced by the pressure needle. Its working process includes steps such as sample placement and parameter setting, with smooth connection between each step. In practical tests, the device shows obvious advantages: at a heating rate of 12℃/6 min, the actual heating rate ranges from (11.9~12.1)℃/6 min, and the temperature indication error is (-0.1~0.2)℃; at a heating rate of 5℃/6min, the actual heating rate is in the range of (4.9~5.1)℃/6 min, and the temperature indication error is (-0.1~0.2)℃, all meeting the technical requirements. Through analysis, the standard uncertainty of temperature indication error is 0.067℃, and the standard uncertainty of heating rate error is 0.091℃/h. The innovation of this research lies in the proposal of a dynamic heating calibration method, optimization of dynamic acquisition strategy, and integration of intelligent calibration algorithms with automated processes, which can support synchronous calibration of multiple temperature points and multiple sample stations. This device effectively solves the problems existing in current calibration methods, realizes synchronous dynamic and accurate measurement of temperature and heating rate, provides a reliable guarantee for material thermal performance testing, and plays an important role in fields such as material research and development and quality control.

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苏彩山,史盼敬,张帅星,孙鹏.基于动态测试的维卡软化温度测定仪校准装置研制[J].电子测量技术,2026,49(4):81-86

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  • 在线发布日期: 2026-04-16
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